Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methoxyethanol → 5-(2-Methoxy-ethoxy)-2-nitro-4-pyrrol-1-yl-phenylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methoxyethanol | HCID 8019 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 5-Chloro-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548859 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 5-(2-Methoxy-ethoxy)-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548743 | — |
반응 단계
The title compound was prepared from 5-chloro-2-nitro-4-pyrrol-1-yl-phenylamine (Example F3) (1.01 g, 4 mmol), 2-methoxyethanol (1.58 mL, 20 mmol) and KOH (316 mg, 4.8 mmol) in DMSO (5 mL) according to the general procedure E. Obtained as an orange solid (870 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06548495B2 |
| 출처 데이터셋 | uspto-grants-2003_04 |
| ORD ID | ord-9e9db5af966b4cfca83cab6f3020956a |
| 출처 메모 | uspto-grants-2003_04 |