Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | 5-Chloro-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548859 | — |
| 용매 | Dimethyl Sulfoxide | HCID 679 | — |
| 생성물 | 5-Methoxy-2-nitro-4-pyrrol-1-yl-phenylamine | HCID 18548717 | — |
반응 단계
The title compound was prepared from 5-chloro-2-nitro-4-pyrrol-1-yl-phenylamine (Example F3) (5.94 g, 25 mmol), methanol (25 mL) and KOH (1.98 g, 30 mmol) in DMSO (25 mL) according to the general procedure E. Obtained as an orange solid (5.88 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06548495B2 |
| 출처 데이터셋 | uspto-grants-2003_04 |
| ORD ID | ord-e6ee15db5ebc44d9980b62679a2b0bb5 |
| 출처 메모 | uspto-grants-2003_04 |