2,5-Dimethoxytetrahydrofuran → HCID 18548859, 화합물

HRID 1266738

반응식

HRID 1266738 반응식
[Cl:1][C:2]1[C:3]([NH2:12])=[CH:4][C:5]([N+:9]([O-:11])=[O:10])=[C:6]([NH2:8])[CH:7]=1.CO[CH:15]1[CH2:19][CH2:18][CH:17](OC)O1>CC(O)=O>[Cl:1][C:2]1[C:3]([N:12]2[CH:15]=[CH:19][CH:18]=[CH:17]2)=[CH:4][C:5]([N+:9]([O-:11])=[O:10])=[C:6]([NH2:8])[CH:7]=1

참가 물질

4

반응물 2

HCID 790982,5-DimethoxytetrahydrofuranHCID 54842901,4-Benzenediamine, 2-chloro-5-nitro-

생성물 1

HCID 18548859HCID 18548859, 화합물

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

The title compound was prepared from 5-chloro-2-nitro-1,4-phenylenediamine [CAS-no. 26196-45-2] (4.69 g, 25 mmol), 2,5-dimethoxytetrahydrofuran (4.2 mL, 32.5 mmol) in HOAc (150 mL) at 95° C. for 2 h according to the general procedure F. Obtained as a red solid (4.10 g).

출처 및 근거

ORD 기록
ord-7446e496d10f423bb939ca3d2ce1e20b
출처 데이터셋
uspto-grants-2003_04
특허 번호
US06548495B2

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