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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1267140생성일: 2026년 10월 26일

Hydrochloric Acid → HCID 86591308, 화합물

https://huagongshe.com/reaction/1267140

반응식

참여 물질

역할이름HCID투입량
반응물Hydrochloric AcidHCID 313—
반응물4'-Trifluoromehtyl-biphenyl-2-carboxylic acid [4-[4-(3-cyano-benzyl)-piperazin-1-yl]-phenyl]-amideHCID 9807315—
용매Ethyl AcetateHCID 8857—
생성물HCID 86591308HCID 86591308—

반응 단계

To a solution of 4′-trifluoromehtyl-biphenyl-2-carboxylic acid [4-[4-(3-cyano-benzyl)-piperazin-1-yl]-phenyl]-amide (0.2 g) in AcOEt (25 mL) was added 1N hydrochloric acid (0.9 mL) and the resulting solution was stirred at room temperature for 1.5 hours. The solution was then evaporated to dryness and the solid was recrystallized from AcOEt/hexane to give the title compound (0.18 g) as a white power.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06552022B1
출처 데이터셋uspto-grants-2003_04
ORD IDord-52e919eeb25e4b04bcc1d41f968ca2f9
출처 메모uspto-grants-2003_04