Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3-Dimethylaniline → HCID 20481270, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3-Dimethylaniline | HCID 6893 | — |
| 반응물 | 2-(chloromethyl)-4,5-dihydro-1H-imidazole hydrochloride | HCID 2760928 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 20481270 | HCID 20481270 | 77% |
반응 단계
31 g of 2-chloromethyl-2-imidazoline hydrochloride and 48.4 g of 2,3-dimethylaniline are refluxed for 5 hours in 65 ml of absolute ethanol. After cooling, the crystallised substance is collected by suction and recrystallised from water, affording 36 g (77% yield) of the final product with a melting point of 242° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04254133 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-e06acf45d0b04201b442b52954b92b8f |
| 출처 메모 | uspto-grants-1981_03 |