Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hexamethylphosphoramide → 1-Ethoxyethyl 4-(hexadecylamino)benzoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hexamethylphosphoramide | HCID 12679 | — |
| 반응물 | Ethane, 1-chloro-1-ethoxy- | HCID 23478 | — |
| 반응물 | Cetaben Sodium | HCID 23703815 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-Ethoxyethyl 4-(hexadecylamino)benzoate | HCID 23457774 | — |
반응 단계
A mixture of 22.0 g. of ethyl 1-chloroethyl ether, 77.0 g. of sodium 4-(hexadecylamino)benzoate and 250 ml. of hexamethylphosphoramide is stirred at 20° C. for 24 hours. After slow addition of water to the crystallization point and standing for 3 hours, the acetal ester is collected on a filter.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04254138 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-d2f27402a5184963a1bbf7e778f3be30 |
| 출처 메모 | uspto-grants-1981_03 |