Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Stearic Acid → N-(2-((2-hydroxyethyl)amino)ethyl)stearamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Stearic Acid | HCID 5281 | — |
| 반응물 | N-(2-Hydroxyethyl)ethylenediamine | HCID 8112 | — |
| 생성물 | N-(2-((2-hydroxyethyl)amino)ethyl)stearamide | HCID 8838 | — |
반응 단계
The dehydration condensation reaction of stearic acid with N-hydroxyethyl ethylene diamine was carried out, and the reaction product was hydrolyzed and distilled to give N-stearoyl-N′-hydroxyethyl ethylene diamine. It was dissolved in ethanol, and 1.1-fold equivalents (based on the amine) of formalin was added dropwise thereto under reflux, then 1.1-fold equivalents (based on the amine) of formic acid was added dropwise thereto, and the mixture was aged for 5 hours. The reaction product was further quaternarized with methyl chloride to give N-stearoylaminoethyl-N-hydroxyethyl-N,N-dimethyl ammonium chloride.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07202203B2 |
| 출처 데이터셋 | uspto-grants-2007_04 |
| ORD ID | ord-a4914ae876964d8cb2d0e43829edd21a |
| 출처 메모 | uspto-grants-2007_04 |