4-Chloro-1-naphthol → 4-Chloro-2-[(2-chlorophenyl)-piperidin-1-yl-methyl]-naphthalen-1-ol

반응식

[Cl-].[Cl:2][C:3]1[CH:15]=[CH:14][CH:13]=[CH:12][C:4]=1[CH:5]=[N+:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1.[Cl:16][C:17]1[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[C:20]([OH:27])=[CH:19][CH:18]=1>>[Cl:16][C:17]1[C:26]2[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=2)[C:20]([OH:27])=[C:19]([CH:5]([C:4]2[CH:12]=[CH:13][CH:14]=[CH:15][C:3]=2[Cl:2])[N:6]2[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]2)[CH:18]=1

참가 물질

반응물 2

HCID 117874-Chloro-1-naphthol

HCID 179587471-(2-Chloro-benzylidene)-piperidinium chloride

생성물 1

HCID 101781914-Chloro-2-[(2-chlorophenyl)-piperidin-1-yl-methyl]-naphthalen-1-ol

실험 절차

The preparation was carried out in accordance with general synthesis instructions 4 from 1-(2-chloro-benzylidene)-piperidinium chloride and 4-chloro-1-naphthol.

출처 및 근거

ORD 기록: ord-2c2eeeda18774c958dfcfe3584befc7f
출처 데이터셋: uspto-grants-2007_04
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07202242B2

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