Di-n-butyldilauryltin → Azelaic Acid

반응식

SN=[C:3]=[O:4].[C:5]([O-:18])(=[O:17])[CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]CCCC.C([O-])(=[O:31])CCCCCCCCCCC.C([Sn+2]CCCC)CCC>>[C:3]([OH:4])(=[O:31])[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][C:5]([OH:18])=[O:17]

참가 물질

반응물 2

HCID 9809426Di-n-butyldilauryltin

HCID 22024120Mercaptoisocyanate

생성물 1

HCID 2266Azelaic Acid

반응 조건

온도: 100 °C

실험 절차

About 50 grams of the mercaptoisocyanate solution prepared in Example 1 along with 0.01 g of dibutyltin dilaurate should be added to about 40 grams of the above prepared polyester and heated for about 3 hours at 100° C. to form a polyester having reactive mercapto groups.

후처리

customto form a polyester having reactive mercapto groups

출처 및 근거

ORD 기록: ord-fcba6d3055e5486d9819cb4c7188a1b3
출처 데이터셋: uspto-grants-1981_03
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04255298

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