Methylamine → 2-(4-methoxyphenyl)-N-methylacetamide

HRID 1272061

반응식

HRID 1272061 반응식
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][C:10](Cl)=[O:11])=[CH:5][CH:4]=1.[CH3:13][NH2:14]>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][C:10]([NH:14][CH3:13])=[O:11])=[CH:5][CH:4]=1

참가 물질

3

반응물 2

HCID 6329MethylamineHCID 27346884-Methoxyphenylacetyl chloride

생성물 1

HCID 32645502-(4-methoxyphenyl)-N-methylacetamide

실험 절차

was prepared from 4-methoxyphenylacetic acid chloride and methylamine following Method B. 1H NMR (300 MHz, CDCl3) δ 7.14 (d, 2H, J=8.67 Hz), 6.86 (d, 2H, J=8.67 Hz), 3.78 (s, 3H), 3.49 (s, 2H), 2.72 (d, 3H, J=4.71 Hz). LCMS (ESI+) [M+H]/z Calc'd 180, found 180.

출처 및 근거

ORD 기록
ord-d7edd9b82e704228bf097a53b0a08b93
출처 데이터셋
uspto-grants-2007_04
특허 번호
US07208500B2

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