돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 127365생성일: 2026년 10월 25일

4,4'-Bis(dimethylamino)diphenylamine → 3-[4-(Diethylamino)-2-methylphenyl]-3-{bis[4-(dimethylamino)phenyl]amino}phthalide

https://huagongshe.com/reaction/127365

반응식

참여 물질

역할이름HCID투입량
반응물4,4'-Bis(dimethylamino)diphenylamineHCID 69473—
반응물2-(4-(Diethylamino)-2-methylbenzoyl)benzoic acidHCID 104335—
생성물3-[4-(Diethylamino)-2-methylphenyl]-3-{bis[4-(dimethylamino)phenyl]amino}phthalideHCID 1551933354%

반응 단계

Following a procedure similar to that described in Example 4 but employing 3.1 g of 2-[4-(diethylamino)-2-methylbenzoyl]benzoic acid and 3.0 g of 4,4'-bis(dimethylamino)diphenylamine there was obtained 2.95 g of 3-[4-(diethylamino)-2-methylphenyl]-3-{bis[4-(dimethylamino)phenyl]amino}phthalide, m.p. 67°-83° C. A toluene solution of the product contacted with acidic clay or phenolic resin developed a black-colored image.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04255577
출처 데이터셋uspto-grants-1981_03
ORD IDord-addf0cc382fb4746827f1a64f5e57980
출처 메모uspto-grants-1981_03