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Methanol → 2,5-Difluoropyridin-4-amine

HRID 1274725
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HRID 1274725 반응식
CO.[NH2:3][C:4]1[C:9](Cl)=[C:8]([F:11])[N:7]=[C:6](Cl)[C:5]=1[F:13]>[C].[Pd].C(N(CC)CC)C>[NH2:3][C:4]1[C:5]([F:13])=[CH:6][N:7]=[C:8]([F:11])[CH:9]=1
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참가 물질

5

반응물 2

HCID 887MethanolHCID 221211852,5-Dichloro-3,6-difluoropyridin-4-amine

생성물 1

HCID 221211752,5-Difluoropyridin-4-amine수율 90.8%

시약·촉매·용매 2

HCID 178418390HCID 178418390, 화합물촉매HCID 8471Triethylamine용매

실험 절차

To 40 ml of methanol were added 4.5 g of 4-amino-2,5-dichloro-3,6-difluoropyridine and 4.5 g of triethylamine together with 0.40 g of 10% palladium carbon, and the mixture was hydrogenated at 50° C. for 12 days. The catalyst was separated by filtration, and the solvent and the like were distilled off under reduced pressure. To the residue was added 100 ml of chloroform, and the mixture was washed with 10 ml of distilled water. The chloroform layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure. To the residue were added 1.5 g of triethylamine, 0.35 g of 10% palladium on carbon, and 30 ml of methanol, and the mixture was hydrogenated at 50° C. for 41 hours. The catalyst was separated by filtration, and the solvent and the like were distilled off under reduced pressure. To the residue was added 100 ml of chloroform, and the mixture was washed with 10 ml of distilled water. The chloroform layer was dried over anhydrous magnesium sulfate and concentrated under reduced pressure to obtain 2.67 g of the title compound as precipitate as a colorless solid.

후처리

  1. customThe catalyst was separated by filtration
  2. distillationthe solvent and the like were distilled off under reduced pressure
  3. additionTo the residue was added 100 ml of chloroform
  4. washthe mixture was washed with 10 ml of distilled water
  5. dry with materialThe chloroform layer was dried over anhydrous magnesium sulfate
  6. concentrationconcentrated under reduced pressure
  7. additionTo the residue were added 1.5 g of triethylamine, 0.35 g of 10% palladium on carbon, and 30 ml of methanol
  8. waitthe mixture was hydrogenated at 50° C. for 41 hours
  9. customThe catalyst was separated by filtration
  10. distillationthe solvent and the like were distilled off under reduced pressure
  11. additionTo the residue was added 100 ml of chloroform
  12. washthe mixture was washed with 10 ml of distilled water
  13. dry with materialThe chloroform layer was dried over anhydrous magnesium sulfate
  14. concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록
ord-04aafa0d9de14b7abdb44bc11711046e
출처 데이터셋
uspto-grants-2000_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06156903

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