Sulfuric Acid → HCID 9951009, 화합물

HRID 1275781노트

반응식

HRID 1275781 반응식
[C:1]1([C:7]2([OH:19])[C:15]3[S:16][CH:17]=[CH:18][C:14]=3[C:13]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]2=3)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C[O:21][C:22](=[O:45])[C@H:23]([C@@H:42]([CH3:44])O)[NH:24]C(OCC1C2C=CC=CC=2C2C1=CC=CC=2)=O.OS(O)(=O)=O>FC(F)(F)C(O)=O>[C:1]1([C:7]2([O:19][C@H:42]([CH3:44])[C@@H:23]([C:22]([OH:45])=[O:21])[NH2:24])[C:15]3[S:16][CH:17]=[CH:18][C:14]=3[C:13]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]2=3)[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

5

반응물 3

HCID 1118Sulfuric AcidHCID 11164107HCID 11164107, 화합물HCID 22117572HCID 22117572, 화합물

생성물 1

HCID 9951009HCID 9951009, 화합물

시약·촉매·용매 1

HCID 6422Trifluoroacetic acid촉매

실험 절차

from 8-phenyl-8H-indeno[2,1-b]thiophen-8-ol (Example 1pp) and Nα -(9-fluorenylmethoxycarbonyl)-L-threonine methyl ester following method A, using trifluoroacetic acid as catalyst in place of H2SO4 ;

출처 및 근거

ORD 기록
ord-37a7253edec84ee9aa88d8dd55eab17d
출처 데이터셋
uspto-grants-2000_12
특허 번호
US06162824

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