Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Bromide → 1-(Phenylmethyl)-1H-1,2,4-triazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Bromide | HCID 7498 | — |
| 반응물 | 1H-1,2,4-Triazole | HCID 9257 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 1-(Phenylmethyl)-1H-1,2,4-triazole | HCID 22458 | — |
반응 단계
A mixture of 34.2 parts by weight of benzyl bromide, 13.8 parts by weight of 1,2,4-triazole and 41.4 parts by weight of potassium carbonate in 150 parts by weight of acetonitrile is refluxed for 10 hours while stirring. The mixture is filtered and the filtrate is evaporated to dryness and recrystallized from a mixture of toluene and cyclohexane. There is obtained 21 parts by weight of 1-benzyl-1,2,4-triazole; m.p.: 58° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04256754 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-26e929fcdfca4b17826444a9104df6a9 |
| 출처 메모 | uspto-grants-1981_03 |