Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dichloromethane → 5-Chloro-2-methoxybenzoyl chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dichloromethane | HCID 6344 | — |
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 5-Chloro-N-{2-[4-(2-hydroxyethyl)phenyl]ethyl}-2-methoxybenzamide | HCID 23453115 | — |
| 생성물 | 5-Chloro-2-methoxybenzoyl chloride | HCID 12384176 | — |
| 생성물 | 4-(2-Hydroxyethyl)-phenethylamine | HCID 21831841 | — |
반응 단계
The 2-{4-[2-(5-chloro-2-methoxybenzamido)-ethyl]-phenyl}-ethanol (oil) used as starting material is obtained by the acylation of 2-[4-(2-aminoethyl)-phenyl]-ethanol (oil) with 5-chloro-2-methoxybenzoyl chloride in anhydrous methylene chloride in the presence of triethylamine as acid acceptor.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04278680 |
| 출처 데이터셋 | uspto-grants-1981_07 |
| ORD ID | ord-3f3d65af07e448f68338a26cfa66dc69 |
| 출처 메모 | uspto-grants-1981_07 |