Ethyl butyrate → Ethyl 2-formylbutanoate

HRID 1277739

반응식

HRID 1277739 반응식
[C:1]([O:6][CH2:7][CH3:8])(=[O:5])[CH2:2][CH2:3][CH3:4].[CH3:9][O-:10].[Na+]>>[CH2:7]([O:6][C:1](=[O:5])[CH:2]([CH:9]=[O:10])[CH2:3][CH3:4])[CH3:8]

참가 물질

3

반응물 2

HCID 7762Ethyl butyrateHCID 10942334Sodium Methoxide

생성물 1

HCID 289299Ethyl 2-formylbutanoate수율 85%

실험 절차

1200 g Ethyl butyrate was reacted with 130 g 85% sodium methylate substantially as in Example 1 to produce 245 g 2-formylbutyric acid ethyl ester (85% yield) boiling at 60°-64° C./14 torr. n20D =1.4300.

출처 및 근거

ORD 기록
ord-181df39d622c4e2b8777a894277e77d5
출처 데이터셋
uspto-grants-1981_07
특허 번호
US04278808

연결된 노트

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