HCID 54271580, 화합물 → HCID 23452590, 화합물

HRID 1278042

반응식

HRID 1278042 반응식
[CH2:1]([N:8]1[CH2:12][CH2:11][CH2:10][C:9]1=[CH:13][C:14]1C=[CH:18][C:17]([O:20][CH3:21])=[C:16]([O:22][CH3:23])[CH:15]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1>C(O)C.[Pt].[H][H]>[CH2:1]([N:8]1[CH2:12][CH2:11][CH2:10][CH:9]1[C:13]1[CH:14]=[CH:15][C:16]([O:22][CH3:23])=[C:17]([O:20][CH3:21])[CH:18]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

4

반응물 1

HCID 54271580HCID 54271580, 화합물

생성물 1

HCID 23452590HCID 23452590, 화합물

시약·촉매·용매 2

HCID 178506450HCID 178506450, 화합물촉매HCID 702Ethanol용매

실험 절차

Dissolve 3 g of 1-benzyl-2-(3,4-dimethoxybenzylidene)pyrrolidine in ethanol and hydrogenate with platinum/hydrogen. Distil the hydrogenated product under a vacuum to obtain 2.3 g (77% of theory) of title compound (b.p. 173° at 0.007 mm of Hg).

후처리

  1. customDistil the hydrogenated product under a vacuum

출처 및 근거

ORD 기록
ord-7d1f95ee81a54e4d90dcedf91fe6275f
출처 데이터셋
uspto-grants-1981_07
특허 번호
US04279918

연결된 노트

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