Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 54229427, 화합물 → 4-[(1-Methylpyrrolidin-2-yl)methyl]aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 54229427 | HCID 54229427 | — |
| 촉매 | HCID 178506450 | HCID 178506450 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-[(1-Methylpyrrolidin-2-yl)methyl]aniline | HCID 13186904 | — |
반응 단계
Reduce 8.5 g of 1-methyl-2-(4-nitrobenzylidene)pyrrolidine in ethanol with platinum/hydrogen. Remove the catalyst and solvent and recrystallize from n-hexane to obtain 3.6 g (49% of theory) of title compound (m.p. 59° to 61°).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04279918 |
| 출처 데이터셋 | uspto-grants-1981_07 |
| ORD ID | ord-f681424255904487938adf5da61e69e1 |
| 출처 메모 | uspto-grants-1981_07 |