HCID 53833314, 화합물 → HCID 23452593, 화합물

HRID 1278048

반응식

HRID 1278048 반응식
[Br:1][C:2]1[CH:14]=[CH:13][C:5]([CH:6]=[C:7]2[CH2:11][CH2:10][CH2:9][N:8]2[CH3:12])=[CH:4][CH:3]=1>C(O)C.[Pt].[H][H]>[Br:1][C:2]1[CH:14]=[CH:13][C:5]([CH2:6][CH:7]2[CH2:11][CH2:10][CH2:9][N:8]2[CH3:12])=[CH:4][CH:3]=1

참가 물질

4

반응물 1

HCID 53833314HCID 53833314, 화합물

생성물 1

HCID 23452593HCID 23452593, 화합물

시약·촉매·용매 2

HCID 178506450HCID 178506450, 화합물촉매HCID 702Ethanol용매

실험 절차

Hydrogenate 21.5 g of 2-(4-bromobenzylidene)-1-methylpyrrolidine in 400 ml of ethanol with platinum on activated charcoal/hydrogen. Filter out the catalyst, concentrate the filtrate and distil the residue to obtain 18.5 g (85% of theory) of the title compound (b.p. 70° at 0.001 mm of Hg).

후처리

  1. filtrationFilter out the catalyst
  2. concentrationconcentrate the filtrate
  3. customdistil the residue

출처 및 근거

ORD 기록
ord-26f51f375edd4c238f0e1cedb920edf8
출처 데이터셋
uspto-grants-1981_07
특허 번호
US04279918

연결된 노트

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