Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Trimethyl phosphite → Allyl dimethylphosphono-acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Trimethyl phosphite | HCID 8472 | — |
| 반응물 | Allyl chloroacetate | HCID 76206 | — |
| 생성물 | Allyl dimethylphosphono-acetate | HCID 13267138 | 70.5% |
반응 단계
191 g of trimethylphosphite were added dropwise under stirring to 188 g of allyl chloroacetate (21/2 h) preliminarly heated to 118°. The reaction mixture was kept at this temperature for 4h, whereupon it was subjected to a distillation to give 205 g of allyl dimethylphosphono-acetate, b.p. 118°/0.1 Torr.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04280934 |
| 출처 데이터셋 | uspto-grants-1981_07 |
| ORD ID | ord-bfd22400082947e1a99bb5f860c160ea |
| 출처 메모 | uspto-grants-1981_07 |