1-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-one → HCID 11299190, 화합물

HRID 1278196노트

반응식

HRID 1278196 반응식
[NH2:1][C:2]1[C:6]([Cl:7])=[CH:5][NH:4][N:3]=1.CN(C)[CH:10]=[CH:11][C:12]([C:14]1[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=1)=O>C(O)(=O)C>[Cl:7][C:6]1[CH:5]=[N:4][N:3]2[C:12]([C:14]3[CH:15]=[N:16][CH:17]=[CH:18][CH:19]=3)=[CH:11][CH:10]=[N:1][C:2]=12

참가 물질

4

반응물 2

HCID 5670331-(3-Pyridyl)-3-(dimethylamino)-2-propen-1-oneHCID 178509265HCID 178509265, 화합물

생성물 1

HCID 11299190HCID 11299190, 화합물

시약·촉매·용매 1

HCID 176Acetic Acid용매

실험 절차

As for Example 2, 3-amino-4-chloropyrazole is heated at reflux temperature for 6 hours with 3-dimethylamino-1-(3-pyridyl)-2-propen-1-one in glacial acetic acid to give the product of the example, m.p. 225°-226° C.

후처리

  1. customto give the product of the example, m.p. 225°-226° C.

출처 및 근거

ORD 기록
ord-62415bafd9c34827954af10cf6c049fb
출처 데이터셋
uspto-grants-1981_07
특허 번호
US04281000

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