Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Formic Acid → N-(4-bromo-3-chlorophenyl)formamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Formic Acid | HCID 284 | — |
| 반응물 | 4-Bromo-3-chloroaniline | HCID 88888 | — |
| 생성물 | N-(4-bromo-3-chlorophenyl)formamide | HCID 12876642 | — |
반응 단계
A mixture of 60.7 g of 4-bromo-3-chloroaniline and 300 ml of 97% formic acid was refluxed for four hours. The resulting mixture was poured over ice and filtered. The solid was washed with water and recrystallized from 3/1 v/v ether/hexane to give N-(4-bromo-3-chlorophenyl)formamide (4A), as a tan solid, mp: 110°-113° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04257805 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-24bdf791f3ff45c995d594be119df269 |
| 출처 메모 | uspto-grants-1981_03 |