Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Acetylpyridine → 3-Dimethylamino-1-(2-pyridyl)prop-2-en-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Acetylpyridine | HCID 14286 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 생성물 | 3-Dimethylamino-1-(2-pyridyl)prop-2-en-1-one | HCID 566993 | — |
반응 단계
A mixture of 25 g. of 2-acetylpyridine and 35 ml. of N,N-dimethylformamide dimethylacetal is refluxed for 16 hours. The mixture is cooled and filtered to give 3-dimethylamino-1-(2-pyridyl)-2-propen-1-one as crystals, m.p. 127°-130° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04281000 |
| 출처 데이터셋 | uspto-grants-1981_07 |
| ORD ID | ord-fba50ffebeec490ab54d32fcab05d345 |
| 출처 메모 | uspto-grants-1981_07 |