Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrazine → 1-Cyclohexyl-1-phenyl-hydrazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrazine | HCID 9321 | — |
| 반응물 | N-Cyclohexylaniline | HCID 74567 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 반응물 | N-Cyclohexyl-N-phenylnitrous amide | HCID 23471014 | — |
| 생성물 | 1-Cyclohexyl-1-phenyl-hydrazine | HCID 12866328 | — |
반응 단계
N-Cyclohexyl-N-nitrosoaniline, prepared from N-cyclohexylaniline by the method described in Example 1 was subsequently reduced to the hydrazine by the lithium aluminum hydride method described in Example 4. 1-Cyclohexyl-1-phenyl hydrazine distilled at 120°-150° C./0.2 mm.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04258059 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-1359a50870784657a2321d5ed8fa712e |
| 출처 메모 | uspto-grants-1981_03 |