Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dioctadecylamine → HCID 20433003, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dioctadecylamine | HCID 66989 | — |
| 반응물 | Ethyl 4-bromobutyrate | HCID 76300 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | HCID 20433003 | HCID 20433003 | 58.2% |
반응 단계
A solution of dioctadecylamine (5.2 g., 0.01 mole), ethyl 4-bromobutyrate (1.95 g., 0.01 mole) and toluene (50 ml.) is heated at reflux for sixteen hours, then cooled and concentrated in vacuo to a semi-solid oil. The oil is triturated with ethylacetate, filtered, and the filtrate washed with water, then dried (Na2SO4). Removal of the solvent gives the product as an oil (3.7 g.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04258061 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-24c64bf11f244c4e8505596e5ea82237 |
| 출처 메모 | uspto-grants-1981_03 |