Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dioctadecylamine → 1-(Dioctadecylamino)methyl-4-cyanobenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dioctadecylamine | HCID 66989 | — |
| 반응물 | 4-(Bromomethyl)benzonitrile | HCID 86996 | — |
| 용매 | Chloroform | HCID 6212 | — |
| 생성물 | 1-(Dioctadecylamino)methyl-4-cyanobenzene | HCID 20432987 | 97.5% |
반응 단계
Dioctadecylamine (26.0 g., 0.05 M), α-bromo-p-tolunitrile (4.9 g., 0.025 M) and chloroform (500 ml.) are stirred at room temperature for 24 hours. The precipitate of dioctadecylamine hydrobromide is filtered off and the filtrate concentrated under reduced pressure. The residue is slurried in methanol, filtered, and evaporated to give 1-(dioctadecylamino)methyl-4-cyanobenzene (15.5 g., 97.5% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04258061 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-5ed02cd3ec794e669594e5566a0b3dfc |
| 출처 메모 | uspto-grants-1981_03 |