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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 127995생성일: 2026년 10월 26일

Dioctadecylamine → 1-(Dioctadecylamino)methyl-4-cyanobenzene

https://huagongshe.com/reaction/127995

반응식

참여 물질

역할이름HCID투입량
반응물DioctadecylamineHCID 66989—
반응물4-(Bromomethyl)benzonitrileHCID 86996—
용매ChloroformHCID 6212—
생성물1-(Dioctadecylamino)methyl-4-cyanobenzeneHCID 2043298797.5%

반응 단계

Dioctadecylamine (26.0 g., 0.05 M), α-bromo-p-tolunitrile (4.9 g., 0.025 M) and chloroform (500 ml.) are stirred at room temperature for 24 hours. The precipitate of dioctadecylamine hydrobromide is filtered off and the filtrate concentrated under reduced pressure. The residue is slurried in methanol, filtered, and evaporated to give 1-(dioctadecylamino)methyl-4-cyanobenzene (15.5 g., 97.5% yield).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04258061
출처 데이터셋uspto-grants-1981_03
ORD IDord-5ed02cd3ec794e669594e5566a0b3dfc
출처 메모uspto-grants-1981_03