Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroxyamine hydrochloride → Hydrochloric Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroxyamine hydrochloride | HCID 443297 | — |
| 반응물 | 3-Ethyl-3-n-butyl-12-phenyl-1-aza-1,5,9-cyclododecatriene | HCID 54523241 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | 1-Phenyl-10-ethyl-10-n-butyl-1,11-diaminoundecane | HCID 20436092 | — |
| 생성물 | 2-Ethyl-2-n-butyl-11-phenyl-11-amino-undeca-4,8-dienal-oxime | HCID 73678919 | — |
반응 단계
Reaction of 3-ethyl-3-n-butyl-12-phenyl-1-aza-1,5,9-cyclododecatriene with hydroxylamine hydrochloride, in the presence of hydrochloric acid and water, to 2-ethyl-2-n-butyl-11-phenyl-11-amino-undeca-4,8-dienal-oxime, and hydrogenation of this to yield 1-phenyl-10-ethyl-10-n-butyl-1,11-diaminoundecane; b.p. 155°-158° C./5 Pa; nD20 =1.5045.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04258176 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-bc27ecb4f0ac4fd6b339612ca059bddf |
| 출처 메모 | uspto-grants-1981_03 |