Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydrazinopyridine → HCID 74054436, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydrazinopyridine | HCID 78645 | — |
| 반응물 | 9,10-Anthracenedicarboxaldehyde | HCID 81500 | — |
| 촉매 | Acetic Acid | HCID 176 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 74054436 | HCID 74054436 | — |
반응 단계
A suspension of 4.68 g. of 9,10-anthracenedicarboxaldehyde in 200 ml. of ethanol containing 4.37 g. of 2-hydrazinopyridine and 2 drops of acetic acid is stirred and heated under reflux for two hours, then allowed to cool. Collection by filtration and washing with ethanol gives the desired product as an orange solid, which sinters from 267° C. to 272° C. (dec.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04258181 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-64d8e624fdc744e58bc205850743ec0c |
| 출처 메모 | uspto-grants-1981_03 |