Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(2-phenyl-phenylmethyl)-phthalimide → 1-Biphenyl-2-ylmethanamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(2-phenyl-phenylmethyl)-phthalimide | HCID 18426122 | — |
| 용매 | Hydrazine hydrate (1:1) | HCID 24654 | — |
| 생성물 | 1-Biphenyl-2-ylmethanamine | HCID 263366 | 78.9% |
반응 단계
N-(2-Phenyl-phenylmethyl)-phthalimide (6.5 g) in 25 cc of hydrazine hydrate were stirred at room temperature overnight. Ice water was added and the solid separated by filtration. The filtrate was salted out with brine and extracted with ethyl acetate. The ethyl acetate extract was washed with water, dried over magnesium sulfate, filtered and concentrated to dryness to afford 3 g of subtitled product as an oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06451839B1 |
| 출처 데이터셋 | uspto-grants-2002_09 |
| ORD ID | ord-92513ac2ba0f4915b383c24c79517d71 |
| 출처 메모 | uspto-grants-2002_09 |