Benzenepropanoic acid → HCID 131723508, 화합물

HRID 1282516노트

반응식

[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH2:11])[CH:2]([CH3:4])[CH3:3].[C:27](O)(=[O:36])[CH2:28][CH2:29][C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1>>[CH2:1]([N:5]([S:15]([C:18]1[CH:23]=[CH:22][C:21]([N+:24]([O-:26])=[O:25])=[CH:20][CH:19]=1)(=[O:17])=[O:16])[C@H:6]([C:12]([OH:14])=[O:13])[CH2:7][CH2:8][CH2:9][CH2:10][NH:11][C:27](=[O:36])[CH2:28][CH2:29][C:30]1[CH:35]=[CH:34][CH:33]=[CH:32][CH:31]=1)[CH:2]([CH3:4])[CH3:3]

참가 물질

반응물 2

HCID 107Benzenepropanoic acid

HCID 69107391HCID 69107391, 화합물

생성물 1

HCID 131723508HCID 131723508, 화합물수율 81%

실험 절차

Nα-isobutyl-Nα-(4-nitrobenzenesulfonyl)-L-lysine was reacted with dihydrocinnamic acid under the conditions described in example 86 to yield 81% of the desired product.

출처 및 근거

ORD 기록: ord-e871ca5ed8c248488adbcc03dc3ae65a
출처 데이터셋: uspto-grants-2002_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06455587B1

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