Chlorotrimethylsilane → HCID 12472499, 화합물

HRID 1283094노트

반응식

HRID 1283094 반응식
[NH:1]1[CH2:5][CH2:4][NH:3][C:2]1=[S:6].[CH3:7][Si:8]([CH3:11])([CH3:10])Cl.C(N(CC)CC)C>O1CCCC1>[CH3:7][Si:8]([CH3:11])([CH3:10])[N:1]1[CH2:5][CH2:4][NH:3][C:2]1=[S:6]

참가 물질

5

반응물 3

HCID 6397ChlorotrimethylsilaneHCID 8471TriethylamineHCID 2723650Ethylenethiourea

생성물 1

HCID 12472499HCID 12472499, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

30.6 parts by weight of imidazolidine-2-thione were boiled overnight with 54.4 parts by weight of trimethylchlorosilane and 51.5 parts by weight of triethylamine in absolute tetrahydrofurane. The warm suspension was freed of the precipitated triethylamine hydrochloride by filtration, and the filtrate was evaporated and dried n a vacuum desiccator.

후처리

  1. filtrationThe warm suspension was freed of the precipitated triethylamine hydrochloride by filtration
  2. customthe filtrate was evaporated
  3. customdried n a vacuum desiccator

출처 및 근거

ORD 기록
ord-ddd16d1308a0445783f6e24af410a5dd
출처 데이터셋
uspto-grants-1976_08
특허 번호
US03974140

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