Ethyl isothiocyanate → HCID 21519704, 화합물
반응식
[C:1]([C:5]1[CH2:6][CH2:7][NH:8][CH2:9][CH:10]=1)([CH3:4])([CH3:3])[CH3:2].[CH2:11]([N:13]=[C:14]=[S:15])[CH3:12]>O1CCCC1>[CH2:11]([NH:13][C:14]([N:8]1[CH2:7][CH:6]=[C:5]([C:1]([CH3:4])([CH3:3])[CH3:2])[CH2:10][CH2:9]1)=[S:15])[CH3:12]참가 물질
4
실험 절차
In 20 ml. of anhydrous tetrahydrofuran there is dissolved 5.0 grams of 4-t-butyl-1,2,3,6-tetrahydropyridine. Stirring is initiated and there is added 3.14 grams of ethylisothiocyanate in 10 ml. of anhydrous tetrahydrofuran allowing the reaction to run at room temperature. After stirring the reaction mixture for 18 hours, the tetrahydrofuran is evaporated in vacuo to give N-ethyl-4-t-butyl-1,2,3,6-tetrahydro-1-pyridinethiocarboxamide.
후처리
- customto run at room temperature
- stirringAfter stirring the reaction mixture for 18 hours
- customthe tetrahydrofuran is evaporated in vacuo
출처 및 근거
- ORD 기록
- ord-ad7a2e1bbe2747feab55afc80d6d5c0b
- 출처 데이터셋
- uspto-grants-1976_08
- 특허 번호
- US03974283
반응 노트
불러오는 중…