Potassium Hydroxide → N,N'-bis(4-anilinophenyl)-2,12-dimethyl-4,7,10-trithiatridecanediamide

참여 물질

역할	이름	HCID	투입량
반응물	Potassium Hydroxide	HCID 14797	—
반응물	Bis(2-mercaptoethyl) sulfide	HCID 77117	—
반응물	2-Propenamide, 2-methyl-N-(4-(phenylamino)phenyl)-	HCID 162468	—
용매	Ethanol	HCID 702	—
생성물	N,N'-bis(4-anilinophenyl)-2,12-dimethyl-4,7,10-trithiatridecanediamide	HCID 21518137	—

반응 조건

온도	50 °C

반응 단계

Sixty-one grams of 2-mercaptoethyl sulfide was added to a solution of 200 grams of N-(4-anilinophenyl) methacrylamide in 2450 milliliters of ethanol. A solution of 5 grams of potassium hydroxide in 50 milliliters of ethanol was then added, and the mixture was heated at 50°C. for 5 hours. Product began to precipitate after about 2 hours. The mixture was then allowed to cool to room temperature and the solid product was filtered off. The product, after drying, weighed 231.5 grams (89 percent of theory) and melted at 131° to 133.5°C.

출처 및 근거

DOI	10.6084/m9.figshare.5104873.v1
특허 번호	US03975414
출처 데이터셋	uspto-grants-1976_08
ORD ID	ord-2359960700c54f4585be3a0945ea3e63
출처 메모	uspto-grants-1976_08