Formic Acid → Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)

HRID 128359

반응식

HRID 128359 반응식
[CH:1](O)=O.[N:4]1[C:11]([NH2:12])=[N:10][C:8]([NH2:9])=[N:7][C:5]=1[NH2:6]>O.[NH4+].[O-][Mo]([O-])(=O)=O.[O-][Mo]([O-])(=O)=O>[CH4:1].[C:5]1([NH2:6])[N:7]=[C:8]([NH2:9])[N:10]=[C:11]([NH2:12])[N:4]=1.[C:5]1([NH2:6])[N:7]=[C:8]([NH2:9])[N:10]=[C:11]([NH2:12])[N:4]=1

참가 물질

5

반응물 2

HCID 284Formic Acid2회HCID 7955Melamine

생성물 1

HCID 103335Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)

시약·촉매·용매 2

HCID 21895884Azanium bis(dioxido(dioxo)molybdenum)촉매HCID 962Water용매3회

실험 절차

Melamine molybdate was prepared in the presence of formic acid as follows. 10 grams of melamine, 7.30 grams of formic acid, and 250 ml water were dissolved together by refluxing in a 500 ml. round-bottomed flask equipped with a stirrer and water-cooled condenser. 26.95 grams of ammonium dimolybdate was dissolved in 50 ml hot water and then added to the first solution. A white precipitate formed immediately.

후처리

  1. temperatureby refluxing in a 500 ml
  2. customround-bottomed flask equipped with a stirrer
  3. additionadded to the first solution
  4. customA white precipitate formed immediately

출처 및 근거

ORD 기록
ord-665b62c240c949c5a1f5832b9a6977a6
출처 데이터셋
uspto-grants-1981_03
특허 번호
US04259491

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