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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1283764생성일: 2026년 10월 26일

Benzoic Acid → Methyl Benzoate

https://huagongshe.com/reaction/1283764

반응식

참여 물질

역할이름HCID투입량
반응물Benzoic AcidHCID 243—
반응물TriethylamineHCID 8471—
반응물Ethyl 2-methoxycarbonyloxyimino-2-cyanoacetateHCID 54529457—
용매MethanolHCID 887—
생성물Methyl BenzoateHCID 7150—

반응 단계

Benzoic acid (1.22 g) and triethylamine (1.4 ml) are dissolved in methanol (15 ml), and ethyl 2-methoxycarbonyloxyimino-2-cyanoacetate (2.0 g) is added thereto. The resulting mixture is stirred at room temperature for 2 hours and then extracted with ethyl acetate. The extract is treated as in Example A to give methyl benzoate (0.9 g) as an oil.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US03976635
출처 데이터셋uspto-grants-1976_08
ORD IDord-7698f43de44d4c74a53fe4940fadaeaa
출처 메모uspto-grants-1976_08