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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1283766생성일: 2026년 10월 26일

Adipic Acid → Diethyl Adipate

https://huagongshe.com/reaction/1283766

반응식

참여 물질

역할이름HCID투입량
반응물Adipic AcidHCID 196—
반응물TriethylamineHCID 8471—
반응물2-Ethoxycarbonyloxyimino-2-cyanoacetic acid amideHCID 54565650—
용매TetrahydrofuranHCID 8028—
생성물Diethyl AdipateHCID 8844—

반응 단계

To a solution of adipic acid (1.46 g) and triethylamine (2.8 ml) in tetrahydrofuran (30 ml), 2-ethoxycarbonyloxyimino-2-cyanoacetic acid amide (3.7 g) is added, and the resulting mixture is stirred at room temperature for 2 hours. The reaction mixture is treated as in Example A to give diethyl adipate (1.5 g) as an oil.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US03976635
출처 데이터셋uspto-grants-1976_08
ORD IDord-60dc19e927b348b0a8b0c60d1d09524c
출처 메모uspto-grants-1976_08