Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isobutyric Acid → Ethyl 5,9-dimethyl-3,4,8-decatrienoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isobutyric Acid | HCID 6590 | — |
| 반응물 | Dehydrolinalool | HCID 62842 | — |
| 반응물 | Ethyl ortho-acetate | HCID 86598186 | — |
| 생성물 | Ethyl 5,9-dimethyl-3,4,8-decatrienoate | HCID 21515741 | 96% |
반응 단계
A mixture of 65.6 g of ethyl ortho-acetate, 30.4 g of dehydrolinalool and 1.5 g of isobutyric acid was reacted at 130° to 140°C. for 8 hours. Distillation was conducted after the reaction in the same manner as in the preceeding Examples, and a fraction boiling at 92 to 94°C. under 0.5 mm Hg was collected. Ethyl 5,9-dimethyl-3,4,8-decatrienoate was obtained in a yield of 96%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03978100 |
| 출처 데이터셋 | uspto-grants-1976_08 |
| ORD ID | ord-c7c8fa9fee444d038d342260fae3be70 |
| 출처 메모 | uspto-grants-1976_08 |