Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Hydroxide → Acifluorfen sodium
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Acifluorfen | HCID 44073 | — |
| 용매 | Isopropanol | HCID 3776 | — |
| 생성물 | Acifluorfen sodium | HCID 44072 | 87.9% |
반응 단계
5-(2-chloro-4-trifluoromethylphenoxy)-2-nitrobenzoic acid (3.0 g, 0.0083 mole) is dissolved in iso-propyl alcohol (20 ml) and a solution of 50% aqueous sodium hydroxide (0.644 g, 0.0083 mole) is added dropwise and the reaction mixture stirred for 1 hour before removing the solvent and water under vacuum at 0.2 mm overnight to afford 2.8 g of sodium 5-(2-chloro-4-trifluoromethylphenoxy)-2-nitrobenzoate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04259510 |
| 출처 데이터셋 | uspto-grants-1981_03 |
| ORD ID | ord-042ebac77fc7400a9b466bd13adc6bac |
| 출처 메모 | uspto-grants-1981_03 |