Triethylamine → 2-[2-[[4-[(dimethylamino)methyl]-2-pyridinyl]methylsulfanyl]ethylamino]-3-methyl-4H-imidazol-5-one
반응식
[CH3:1][N:2]([CH2:4][C:5]1[CH:10]=[CH:9][N:8]=[C:7]([CH2:11][S:12][CH2:13][CH2:14][NH2:15])[CH:6]=1)[CH3:3].I.[CH3:17][N:18]1[CH2:22][C:21](=[O:23])[N:20]=[C:19]1SC.C(N(CC)CC)C>C(O)C>[CH3:3][N:2]([CH2:4][C:5]1[CH:10]=[CH:9][N:8]=[C:7]([CH2:11][S:12][CH2:13][CH2:14][NH:15][C:19]2[N:18]([CH3:17])[CH2:22][C:21](=[O:23])[N:20]=2)[CH:6]=1)[CH3:1]참가 물질
5
반응물 3
생성물 1
시약·촉매·용매 1
실험 절차
2-(4-(Dimethylaminomethyl)pyrid-2-ylmethylthio)ethylamine (2.25 g), 1-methyl-2-methylthio-imidazolin-4-one hydroiodide (2.71 g) and triethylamine (2.18 g) were refluxed in ethanol (50 ml) for 6 hours.
출처 및 근거
- ORD 기록
- ord-caf0116fc97b4efb95a8ec2d6e9ce637
- 출처 데이터셋
- uspto-grants-1986_01
- 특허 번호
- US04567176
반응 노트
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