Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol, 2-fluoro-2,2-dinitro- → 1-Fluoro-1,1,5-trinitro-3-oxa-5azahexane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol, 2-fluoro-2,2-dinitro- | HCID 28189 | — |
| 반응물 | Acetic acid, trifluoro-, (methylnitroamino)methyl ester | HCID 13352131 | — |
| 생성물 | 1-Fluoro-1,1,5-trinitro-3-oxa-5azahexane | HCID 13352133 | — |
반응 단계
reacting one mole of 2-nitro-2-azapropyl trifluoroacetate with one mole of 2-fluoro-2,2-dinitroethanol in a polar solvent at a temperature of from 0° C. to 40° C. to form 1-fluoro-1,1,5-trinitro-3-oxa-5azahexane, wherein the reaction is run under vacuum to remove trifluoroacetic acid generated by the reaction; and
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04567296 |
| 출처 데이터셋 | uspto-grants-1986_01 |
| ORD ID | ord-45804309d9454f8fb4d6d054f98606be |
| 출처 메모 | uspto-grants-1986_01 |