tert-Butyl mercaptan → 3-(tert-Butylsulfanyl)propanenitrile

반응식

[CH3:1][C:2]([SH:5])([CH3:4])[CH3:3].[C:6](#[N:9])[CH:7]=[CH2:8].C[O-].[Na+]>>[CH3:1][C:2]([S:5][CH2:8][CH2:7][C:6]#[N:9])([CH3:4])[CH3:3]

참가 물질

반응물 3

HCID 6387tert-Butyl mercaptan2회

HCID 7855Acrylonitrile

HCID 10942334Sodium Methoxide

생성물 1

HCID 146643833-(tert-Butylsulfanyl)propanenitrile

실험 절차

β-(2-Methyl-2-propylmercapto)propionitrile was prepared according to the procedure of Example 1 using 2-methyl-2-propanethiol according to the procedure of Example 1 using 2-methyl-2-propanethiol (25.0 g; 0.28 moles), acrylonitrile (14.9 g; 0.28 moles) and sodium methoxide (0.5 g).

출처 및 근거

ORD 기록: ord-6ea73220a2f145b6bf4c39b9a2ea4758
출처 데이터셋: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03984336

반응 노트

불러오는 중…