Acrylonitrile → 3-[(3-Methylphenyl)sulfanyl]propanenitrile

HRID 1287201노트

반응식

[C:1]1([CH3:8])[CH:6]=[CH:5][CH:4]=[C:3]([SH:7])[CH:2]=1.[C:9](#[N:12])[CH:10]=[CH2:11].C[O-].[Na+]>>[CH3:8][C:1]1[CH:2]=[C:3]([S:7][CH2:11][CH2:10][C:9]#[N:12])[CH:4]=[CH:5][CH:6]=1

참가 물질

반응물 3

HCID 7855Acrylonitrile

HCID 79303-Thiocresol

HCID 10942334Sodium Methoxide

생성물 1

HCID 123249263-[(3-Methylphenyl)sulfanyl]propanenitrile

실험 절차

β-(3-Methylphenyl)mercaptopropionitrile was prepared according to the procedure of Example 1 using m-toluenethiol (20.0 g; 0.16 moles), acrylonitrile (8.6 g; 0.16 moles) and sodium methoxide (0.5 g).

출처 및 근거

ORD 기록: ord-d3377dd874f04db3bc958e288899e40d
출처 데이터셋: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03984336

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