Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetone → HCID 178444015, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetone | HCID 180 | — |
| 반응물 | 2-Chloro-4-methylphenyl isothiocyanate | HCID 143529 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 반응물 | Heptanimidamide hydrochloride | HCID 14144282 | — |
| 용매 | Benzene n-pentane | HCID 19707280 | — |
| 생성물 | HCID 178444015 | HCID 178444015 | — |
반응 단계
Following a procedure similar to that described in Example 42 and using 2.3 g. sodium in 250 ml. dry acetone, 16.4 g. heptanamidine hydrochloride, and 16 g. 2-chloro-4-methylphenyl isothiocyanate (b.p. 80°-82°C./0.3 mm.; prepared from 2-chloro-4-methylaniline) in 100 ml. dry acetone there was obtained 1-(2-chloro-4-methylphenyl)-3-(heptanimidoyl)-2-thiourea, m.p. 78°-80°C. (from benzene-n-pentane); hydrochloride (23 g.), m.p. 138°-140°C. (from isopropyl alcohol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03984467 |
| 출처 데이터셋 | uspto-grants-1976_10 |
| ORD ID | ord-b0270527fc824ddfa2752b037e6a82c8 |
| 출처 메모 | uspto-grants-1976_10 |