Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1287489생성일: 2026년 10월 26일
Decane, 1-isothiocyanato- → 8-Chloro 3-(n-decyl) pyrido (1,2-a) 1,3,5-triazine-2,4-dithione
https://huagongshe.com/reaction/1287489
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Decane, 1-isothiocyanato- | HCID 90535 | — |
| 반응물 | 4-Chloro-2-isothiocyanatopyridine | HCID 21508905 | — |
| 생성물 | 8-Chloro 3-(n-decyl) pyrido (1,2-a) 1,3,5-triazine-2,4-dithione | HCID 56607191 | — |
반응 단계
0.511 G. of 4-Chloro-2-pyridyl isothiocyanate and 1.8 g. of n-decylisothiocyanate are combined and heated at 85° C. for 20 hours. The temperature is lowered to 75° C. and continued for 8 days. The reaction mixture is cooled, triturated with ether, filtered, washed with water and dried affording 8-chloro 3-(n-decyl) pyrido (1,2-a) 1,3,5-triazine-2,4-dithione m.p. 153°-155° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US03984549 |
|---|
| 출처 데이터셋 | uspto-grants-1976_10 |
|---|
| ORD ID | ord-e28dbc71cf6e40518f37c7328ca7a664 |
|---|
| 출처 메모 | uspto-grants-1976_10 |
|---|
