Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Naphthol → Ethyl 6-(2-naphthyloxy)hexanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Naphthol | HCID 8663 | — |
| 반응물 | Ethyl 6-bromohexanoate | HCID 117544 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | Ethyl 6-(2-naphthyloxy)hexanoate | HCID 19375098 | — |
반응 단계
Ethyl 6-bromohexanoate and the sodium salt of 2-naphthol are reacted in DMF at 70° to provide ethyl 6-(2-naphthyloxy)hexanoate, which after the usual workup is reduced with lithium aluminum hydride in THF to provide 6-(2-naphthyloxy)hexanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05464865 |
| 출처 데이터셋 | uspto-grants-1995_11 |
| ORD ID | ord-cbe01735c94b4625940887766daee71c |
| 출처 메모 | uspto-grants-1995_11 |