Thionyl Chloride → 4-(2-Cyanoethyl)benzoyl chloride

HRID 1287958노트

반응식

HRID 1287958 반응식
[C:1]([CH2:3][CH2:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](O)=[O:10])=[CH:7][CH:6]=1)#[N:2].S(Cl)([Cl:16])=O>>[C:1]([CH2:3][CH2:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([Cl:16])=[O:10])=[CH:7][CH:6]=1)#[N:2]

참가 물질

3

반응물 2

HCID 24386Thionyl Chloride2회HCID 198791964-(2-Cyanoethyl)benzoic acid

생성물 1

HCID 450817144-(2-Cyanoethyl)benzoyl chloride

실험 절차

A mixture of 17.5 parts of 4-(2-cyanoethyl) benzoic acid and 120 parts of thionyl chloride are refluxed for 15 minutes. The surplus thionyl chloride is then eliminated under reduced pressure and the 4-(2-cyanoethyl) benzoyl chloride is obtained which is liquid at atmospheric temperature.

후처리

  1. temperatureare refluxed for 15 minutes

출처 및 근거

ORD 기록
ord-95030aba77e9410f92b623f38cd26edd
출처 데이터셋
uspto-grants-1976_10
특허 번호
US03987027

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