4-Hydroxybenzaldehyde → HCID 19375134, 화합물

반응식

[OH:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][CH:3]=1.[CH2:10]=[CH:11][CH:12](O)[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17]C>>[CH:11]([CH:12]([O:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=[O:7])=[CH:4][CH:3]=1)[CH2:13][CH2:14][CH2:15][CH2:16][CH3:17])=[CH2:10]

참가 물질

반응물 2

HCID 1264-Hydroxybenzaldehyde

HCID 895601-Nonen-3-ol

생성물 1

HCID 19375134HCID 19375134, 화합물

실험 절차

By the method of example 13, 4-hydroxybenzaldehyde and 1-nonen-3-ol are coupled under Mitsunobu conditions, producing 4-((1-ethenylhexyl)oxy)benzaldehyde. By the methods described in example 1, this benzaldehyde is chain-extended and condensed with glyoxylic acid to provide the title compound as a colorless oil after chromatography, which solidifies on standing giving a colorless solid, mp 46°-50°.

출처 및 근거

ORD 기록: ord-c371c94fadf548abafb111ba822a36b2
출처 데이터셋: uspto-grants-1995_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05464865

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