Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydrazinoethanol → 1-Methyl-2-nitro-5-imidazolecarboxaldehyde-2-hydroxyethylhydrazone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydrazinoethanol | HCID 8017 | — |
| 반응물 | 1-Methyl-2-nitro-1H-imidazole-5-carboxaldehyde | HCID 100390 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 1-Methyl-2-nitro-5-imidazolecarboxaldehyde-2-hydroxyethylhydrazone | HCID 332382 | — |
반응 단계
A solution of 0.300 g. of 2-hydroxyethylhydrazine and 0.4 g. of 1-methyl-2-nitro-5-imidazolecarboxaldehyde in 20 ml. of methanol is allowed to stand for two days. The solid which precipitates is recovered on the filter and washed with water. Yield: 0.245 g., m.p. 138°-140° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US03987053 |
| 출처 데이터셋 | uspto-grants-1976_10 |
| ORD ID | ord-6311266d71494924886e9baa0e9090d5 |
| 출처 메모 | uspto-grants-1976_10 |