Ethyl chloroformate → HCID 68137906, 화합물

반응식

[CH3:1][C:2]1[C:11]2[CH:10]=[CH:9][CH:8]=[C:7]([N+:12]([O-:14])=[O:13])[C:6]=2[N:5]=[C:4]2[CH2:15][CH2:16][NH:17][CH2:18][CH2:19][C:3]=12.[Cl:20][C:21]([O:23][CH2:24][CH3:25])=[O:22]>>[ClH:20].[CH2:24]([O:23][C:21]([N:17]1[CH2:18][CH2:19][C:3]2[C:4](=[N:5][C:6]3[C:7]([N+:12]([O-:14])=[O:13])=[CH:8][CH:9]=[CH:10][C:11]=3[C:2]=2[CH3:1])[CH2:15][CH2:16]1)=[O:22])[CH3:25]

참가 물질

반응물 2

HCID 10928Ethyl chloroformate

HCID 215034751,2,4,5-tetrahydro-11-methyl-7-nitro-3H-azepino[4,5-b]quinoline

생성물 1

HCID 68137906HCID 68137906, 화합물수율 70%

실험 절차

1,2,4,5-Tetrahydro-11-methyl-7-nitro-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester hydrochloride was prepared from 1,2,4,5-tetrahydro-11-methyl-7-nitro-3H-azepino[4,5-b]quinoline and ethyl chloroformate analogous to Example 63.

출처 및 근거

ORD 기록: ord-5d4fc2917bd54f14a698cd0e06815767
출처 데이터셋: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03987047

반응 노트

불러오는 중…