Dimethylamine → HCID 68140352, 화합물

HRID 1288170노트

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[CH2:1]([O:3][C:4]([N:6]1[CH2:20][CH2:19][C:18]2[C:9](=[N:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[C:17]=2[CH3:21])[CH:8]([Cl:22])[CH2:7]1)=[O:5])[CH3:2].[CH3:23][NH:24][CH3:25]>>[ClH:22].[ClH:22].[CH2:1]([O:3][C:4]([N:6]1[CH2:20][CH2:19][C:18]2[C:9](=[N:10][C:11]3[CH:12]=[CH:13][CH:14]=[CH:15][C:16]=3[C:17]=2[CH3:21])[CH:8]([N:24]([CH3:25])[CH3:23])[CH2:7]1)=[O:5])[CH3:2]

참가 물질

반응물 2

HCID 674Dimethylamine

HCID 54025343HCID 54025343, 화합물

생성물 1

HCID 68140352HCID 68140352, 화합물수율 77%

실험 절차

5-Dimethylamino-1,2,4,5-tetrahydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester dihydrochloride was prepared from 5-chloro-1,2,4,5-tetrahydro-11-methyl-3-azepino[4,5-b]quinoline-carboxylic acid ethyl ester and dimethylamine analogous to Example 173.

출처 및 근거

ORD 기록: ord-6fbd92f3fd904a7e891f2bb6c8f2d78e
출처 데이터셋: uspto-grants-1976_10
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US03987047

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